Detection performance of metal powder and summary of detection methods

Metal powder is a fine metal powder, usually made by chemical reduction of metal, mechanical grinding or atomization. They have the properties of many metals, such as high electrical conductivity, high thermal conductivity, corrosion resistance, high temperature performance, etc. Metal powders can be used in a variety of applications, such as the preparation of metal materials in the fields of electronic devices, automobiles, aerospace, construction, metallurgy, etc., and added to coatings, paints, inks, rubber, etc. to increase their electrical conductivity, thermal conductivity, corrosion resistance and other properties. In addition, metal powder is also widely used in powder metallurgy, 3D printing, thermal spraying and other fields.

Detection performance

The following is a table of common properties and detection methods that metal powder needs to detect:

performancedescribeDetection method
Particle size distributionSize and distribution of metal powder particlesLaser particle size analyzer, microscope
chemical compositionThe content and ratio of each element in the metal powderX-ray fluorescence spectroscopy, ICP-MS, chemical analysis
purityPurity and Impurity Content of Metal PowdersICPOES, thermogravimetric analysis, gas chromatography-mass spectrometry
densityDensity and porosity of metal powdersBuoyancy method, mercury intrusion method, microscope
magneticMagnetic Properties of Metal PowdersVibrating sample magnetometer, hysteresis loop test
surface propertiesSurface Morphology, Chemical Reaction and Chemical Composition of Metal PowdersScanning Electron Microscopy, X-ray Photoelectron Spectroscopy, Chemical Analysis

Beichao reminds you: Different metal powders may require different detection methods, and which method to choose depends on the nature of the sample and the required detection accuracy.

Specific detection method

The following is a detailed description of metal powder detection:

  1. Particle size and particle size distribution: measure particle size and particle size distribution by laser particle size analyzer, dynamic light scattering instrument and other instruments.

  2. Density: Measured by hydrometer or gas specific gravity method.

  3. Thermogravimetric analysis: The thermal stability and thermal decomposition temperature of materials can be tested with thermogravimetric analyzer (TGA) or differential thermal analyzer (DSC).

  4. Chemical composition: The commonly used methods are X-ray fluorescence spectroscopy (XRF) and atomic absorption spectroscopy (AAS).

  5. Surface properties: Common surface analysis methods include scanning electron microscopy (SEM), transmission electron microscopy (TEM) and atomic force microscopy (AFM).

  6. Magnetic properties: The magnetic properties of materials are tested with equipment such as superconducting quantum interferometers (SQUIDs) and Hall effect meters.

  7. Conductivity: Instruments such as a four-probe resistance Tester can be used to test the conductivity of a material.

  8. Optical properties: Ultraviolet-visible Spectrophotometer (UV-Vis) and other instruments can be used to test the absorption and transmission spectra of materials, as well as optical properties such as fluorescence spectra.

  9. Mechanical properties: Commonly used mechanical property testing methods include tensile, compression, bending and other experiments, as well as instruments such as material testing machines to test the mechanical properties of materials.

These test methods need to be selected according to the specific metal powder type and properties, and combined with a variety of means for comprehensive analysis.

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