Determination method for solid content of coatings

The solids content of a coating is an important indicator for evaluating the quality of the coating, which indicates the proportion of solids in the paint to the total weight, which is usually determined by the ratio of the weight of the residue after heating and drying to the weight of the sample. Accurate determination of the solids content of coatings is essential for production, R&D and quality control. This article will introduce the standard and operation method of "Paint Solids Determination Method GB1725-79".

 1. Instruments and equipment

The equipment required to determine the solids content of coatings includes glass petri dishes, glass surface dishes, grinding drip bottles, glass dryers, thermometers, balances, and blast ovens. These devices guarantee precision and reliability in the measurement process, especially the accuracy of the balance (inductance of 0.01 grams), which ensures the accuracy of the measurement results.

2. Determination method

The standard provides two main methods of determination, and the appropriate method is selected according to the different types of coatings.

Petri dish method- This is a conventional method for general coatings. First, use a dried Petri dish to preheat it in an oven to remove moisture from it. Then, a certain amount of paint sample is weighed and placed in a weighed Petri dish. Next, the sample is placed in a thermostatic oven and baked at the specified temperature until the sample reaches a constant weight. Multiple weighings are required in the process to ensure that the difference between the two weighings is less than 0.01 grams. This method is easy to use and can be applied to most paint samples.

Surface dish method- For high-viscosity paints (e.g. putty, emulsions, and some types of lacquers), the surface dish method is used. This method requires two surface dishes that are matched to each other, one of which houses the paint sample and the other is reversed and pressed against the sample, ensuring uniform heating of the sample. Similar to the Petri dish method, the sample needs to be baked in a thermostatic oven until it reaches a constant weight. This method is mainly used to process highly viscous coatings.

3. Baking temperature regulations

Different types of coatings have different baking requirements. In order to ensure accurate determination of the solids content, the temperature at which the paint is baked in the oven needs to be adjusted according to the type of paint. For example, nitro paints, perchloroethylene paints, etc., have a baking temperature of 80°C, while some polyester paints and water-based paints have baking temperatures as high as 150°C to 200°C, respectively. These temperature settings ensure that the solids content of different coatings can be precisely determined under the right conditions.

Fourth, the processing of the measurement results

The determination of solids content is usually determined by the average of two parallel tests. If the difference between the two tests exceeds a certain standard (relative error is not more than 3%), the measurement needs to be re-measured. These test results allow for an accurate assessment of the solids content of the coating, helping manufacturers understand the ratio of volatile to solid components in the coating to optimize the production process and product performance.

5. The importance and application of standards

The implementation of the "Paint Solids Determination Method GB1725-79" is of great significance to the coating industry. It provides a unified code of practice for coating production, inspection and quality control, helping to ensure the quality stability of coatings and avoid negative effects on coating performance due to changes in solids content. The implementation of the standard also promotes the research and development and market competitiveness of coating products, and helps enterprises produce coating products that meet quality requirements.

summary

"Coating Solid Content Determination Method GB1725-79" provides a scientific and standardized solid content determination method for the coating industry, which ensures the reliability of coating quality. By using the right instruments and assays, manufacturers and researchers are able to obtain accurate data that supports quality control and improvement of their products. The implementation of this standard has a far-reaching impact on improving the performance and market competitiveness of coating products.


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