Preparation of Graphene Oxide and TPU Composite Films by Coating Machine

In order to improve the dispersibility of GO in organic solvents and improve the barrier properties of TPU films, firstly, graphene oxide (GO) was prepared by the modified Hum-mers method ; then, the excellent performance of isophorone diisocyanate (Isophorone Dissocyanate IPDI) modified GO to prepare functional GO (Functional Graphene Oxide IP-GO ); finally, it was compounded with TPU on a coating machine to prepare IP-GO/TPU composite film, and the effect of IPGO content on IP - Effect of oxygen transmission rate of GO/TPU composite film .

Photo 1 of the composite film of graphene oxide and TPU prepared by the film coating machine

First, weigh 15g of well-dried TPU particles, and after swelling in 60ml of DMF for a period of time, the dissolved TPU is obtained . Then, 0.075g of IP-GO was weighed and added to 20mL DMF . After ultrasonic dispersion for a period of time, it was mixed . After several hours of mechanical stirring, it was left to stand for a period of time to remove the bubbles in the mixture to obtain a uniform Mixture . Finally, a film with a thickness of (0.13±0.01) mm was coated on a film coating machine using a Wet Film Applicator. After the solvent evaporated completely, a 0.5wt% IP-GO/TPU composite film was obtained . The quality of IP-GO was changed , and IPGO / TPU composite films with IP-GO content . Three samples were prepared for each of the above films, and three pure TPU film samples were prepared for comparison.


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